Metallographic Analysis

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🔎 Case Sharing: Semipol for Grinding & Polishing of Silicon-Based Chip End Faces

Objective: Grind and polish the chip end face to a mirror finish, ensuring end face perpendicularity and no edge chipping. Key Challenges: Silicon-based chips are brittle, small in size, and difficult to fix during sample preparation. Material: Silicon-based chip Equipment & Accessories Equipment: Semipol high-precision grinding and polishing machine Accessories: Thin-sheet sample mounting fixture Consumables […]

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🔎 Polishing Preparation Scheme for Niobium-Based Ceramic Coating Samples

Preparing high-temperature oxidation-resistant ceramic coatings on niobium and niobium alloy substrates is a key surface technology to extend their excellent high-temperature strength for applications in oxygen-containing environments. The core challenges in this field lie in resolving the enormous thermal stress caused by the mismatch in thermal expansion coefficients between metals and ceramics, as well as […]

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🔎 Preparation Scheme for 316 Powder Metallurgy Stainless Steel

316 powder metallurgy (PM) stainless steel, leveraging its advantages of corrosion resistance, high strength, and near-net shaping, has been widely applied in scenarios such as automotive engine valve cores, medical device implants, chemical corrosion-resistant valves, offshore platform fasteners, and electronic equipment structural components. The core purpose of its sample preparation is not only to present […]

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🔎 Preparation of Chip Solder Ball Samples

Chip solder balls are small spherical beads made of pure tin or tin alloys. They are used to provide electrical connection and mechanical support between chip packaging and printed circuit boards (PCBs), as well as connections between stacked packages in multi-chip modules (MCMs). In Ball Grid Array (BGA) packaging, solder balls resolve the conflict between […]

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🔎 Preparation Scheme for Cermet Polished Samples

Cermet, also known as ceramic matrix composite, is a multiphase system composed of metals or alloys and one or more ceramic phases. This type of material integrates the excellent toughness and thermal conductivity of the metal phase with the high hardness, wear resistance and heat resistance of the ceramic phase, thus combining the advantages of […]

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🔎 Efficient Preparation Scheme for PCB Samples

As the core carrier of electronic manufacturing, the internal structural quality of PCBs directly determines the reliability of end products. Metallographic section testing is the most robust “quality perspective tool” in the PCB industry, unlocking the “hidden truth” of circuit boards step by step—from sampling, mounting, grinding, polishing to microscopic observation.   Whether it is […]

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🔎 Preparation Scheme for 431 Martensitic Stainless Steel

In the field of materials science, martensitic stainless steel occupies a unique position due to its heat-treatable strengthening property, with 431 steel (Chinese grade: 1Cr17Ni2) being a typical representative. Its performance stems from precise alloy design: 💠 Carbon content (≤0.20%), as interstitial atoms, is the core of martensitic transformation. Quenching after austenitization forms a supersaturated […]

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🔎 BGA Sample Preparation Plan

As electronic products continue to evolve towards miniaturization and high-density integration, ball grid array (BGA) packaging has become the core packaging form for devices such as smartphones and aerospace systems due to its ability to achieve high I/O pin density connections. Although the solder joints between BGA and printed circuit boards (PCBs) are of tiny […]

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🔎 Sample Preparation of Copper Resistance Materials

Copper resistors are by no means simple “conductive components”—their core value stems from their resistance-temperature characteristics and low resistivity advantages, which together underpin their applications across multiple fields.   They serve three core functions: – **Temperature sensing**: Converting temperature into electrical signals; – **Energy transmission**: Acting as “conductive bridges” to reduce circuit losses; – **Circuit […]

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🔎 Analysis of the Rainbow Film Issues in Aluminum Alloy Laser Welding Samples

The aluminum alloy welding samples exhibited the phenomenon of a rainbow film after being exposed to corrosion and cleaning. The pictures show the aluminum alloy welding samples with the rainbow film, and the surface of the sample re-prepared after vacuum impregnation to fill the pores. When there are gaps between the sample and the resin […]

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🔎 Preparation of chalcopyrite samples

Chalcopyrite ore is a type of ore containing chalcopyrite, with the main component being chalcopyrite (chemical formula: CuFeS₂). The theoretical composition includes 34.56% Cu, 30.52% Fe, and 34.92% S. It usually also contains trace elements such as Ag, Au, Tl, Se, Te, and is mostly a mechanical admixture. Sometimes it also contains Ge, Ga, In, […]

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 Preparation of EBSD Samples for Third-Generation Semiconductor Power Devices

Power Devices The third-generation semiconductor power devices are mainly manufactured based on wide-bandgap semiconductor materials such as silicon carbide (SiC) and gallium nitride (GaN), and compared with traditional silicon-based devices, they have significant advantages such as large bandgap width, high breakdown electric field strength, and fast electron saturation drift speed. These characteristics enable the third-generation […]

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Preparation of automotive chip composite material samples

Automotive chips, as the “brain” and “nerve” of automobiles, are leading the intelligent transformation of the automotive industry. With the transformation of automobiles from traditional mechanical products to intelligent mobile terminals, the importance of automotive chips has become increasingly prominent. It not only determines the performance, safety and intelligence level of automobiles, but also becomes […]

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Preparation of microstructure samples of ternary precursor powder for lithium-ion battery cathode materials 

Under the dual pressures of energy shortage and global environmental protection, lithium batteries, with their high energy density and long cycle life, have become the core choice in the fields of energy storage and power. From power station energy storage systems, telecommunications and communication uninterruptible power supplies, to electric vehicles, military and aerospace equipment, the […]

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Preparation of Archaeological Slag Samples

Ancient slag holds multi-dimensional academic value and practical significance. Its importance can be analyzed from various fields such as archaeology, metallurgical technology history, environmental history, and economic history. Slag is the direct product of metallurgical activities. Its chemical composition and physical structure (such as the mineral composition of slag, bubble distribution, and molten state) can […]

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🔎 High-speed steel microstructure preparation

High-speed steel is a type of tool steel with high hardness, high wear resistance and high heat resistance, commonly known as white steel. Its most significant characteristic – red hardness – refers to the ability of the cutting edge to resist softening when the tool is in a red-hot state during high-speed cutting, maintaining a […]

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🔎 Preparation of petroleum pipe material samples

Petroleum pipe materials are key materials in the petroleum and natural gas industry, mainly divided into oil casing, drill pipe and pipeline pipe, each with distinct characteristics and performance. Oil casing: “Guardian” of oil wells, with high strength, good toughness, corrosion resistance, precise dimensions, and stable well wall to prevent collapse. Drill pipe: “Force transmission […]

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🔎 Microscopic sample preparation of high-temperature titanium alloy

👏 High-temperature titanium alloy is a type of titanium alloy that can be safely and reliably used in service environments above 400℃. Due to its ability to maintain high tensile strength at high temperatures, along with excellent thermal stability, good fatigue performance, and good creep resistance, it is mainly used to manufacture discs, blades, intake […]